ANALISIS TERMAL PHASE CHANGE MATERIAL CaCl₂.6H₂O BERBAHAN DASAR LIMBAH CANGKANG TELUR AYAM DENGAN PENAMBAHAN MgCl₂.6H₂O - SrCl₂.6H₂O - CMC

VIDYA EKSA PUTRI HILDA, . (2026) ANALISIS TERMAL PHASE CHANGE MATERIAL CaCl₂.6H₂O BERBAHAN DASAR LIMBAH CANGKANG TELUR AYAM DENGAN PENAMBAHAN MgCl₂.6H₂O - SrCl₂.6H₂O - CMC. Sarjana thesis, UNIVEVRSITAS NEGERI JAKARTA.

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Abstract

Meningkatnya kebutuhan energi telah mendorong pengembangan sistem Thermal Energy Storage (TES) yang efisien dengan menggunakan kalsium klorida heksahidrat (CaCl₂.6H₂O) sebagai Phase Change Material (PCM). Bahan ini memiliki kapasitas penyimpanan energi termal yang baik, meskipun menghadapi tantangan seperti supercooling dan pemisahan fase. Penelitian ini berfokus pada sintesis dan karakteristik dari CaCl₂.6H₂O berbahan limbah cangkang telur ayam menggunakan 5% HCl. Selanjutnya, 20wt% MgCl₂.6H₂O dicampurkan dengan hasil sintesis CaCl₂.6H₂O untuk memperoleh campuran eutektik dengan menyesuaikan suhu transisi fasa sesuai kenyamanan termal di dalam bangunan. 1wt% SrCl₂.6H₂O ditambahkan untuk menekan fenomena supercooling pada campuran eutektik. Kombinasi dengan 0,5wt% CMC digunakan untuk mengatasi pemisahan fasa. Analisis FTIR dan XRD mengonfirmasi tahapan sintesis material berbasis cangkang telur ayam identik dengan parameter referensi. Hasil FTIR menunjukkan munculnya puncak serapan khas yang berkesesuaian dengan struktur molekul kalsium karbonat pada bahan baku, serta keberadaan pita O-H dan kalsium klorida pada fase CaCl₂.2H₂O dan CaCl₂.6H₂O. Sementara itu, data XRD menunjukkan pola difraksi yang identik dengan parameter referensi, menegaskan bahwa material yang terbentuk memiliki kristalinitas tinggi dan minim pengotor. Pengujian termal menggunakan DSC menunjukkan bahwa material hasil sintesis memiliki titik leleh puncak sebesar 26,3°C, yang sesuai untuk aplikasi kenyamanan termal pada dinding bangunan sekitar 22°C–26°C. Meskipun terdapat sedikit penurunan entalpi menjadi 109,3 J/g dibandingkan material standar laboratory grade 123,13 J/g akibat pengaruh viskositas CMC dan tingkat kemurnian bahan baku. Menariknya, penurunan entalpi tersebut lebih efisien dibandingkan material technical grade komersial. Hasil ini membuktikan bahwa cangkang telur ayam berpotensi efektif dan ekonomis untuk pengembangan PCM berkelanjutan di masa depan. Kata Kunci : CaCl₂.6H₂O, cangkang telur ayam, MgCl₂.6H₂O, phase change material (PCM), titik leleh ***** Increasing energy needs have driven the development of efficient Thermal Energy Storage (TES) using calcium chloride hexahydrate (CaCl₂.6H₂O) as a Phase Change Material (PCM). This material has good thermal energy storage capacity, although it faces challenges such as supercooling and phase separation. This study examines the synthesis and characteristics of CaCl₂.6H₂O from chicken eggshell waste using 5% HCl Next, 20 wt% MgCl₂.6H₂O was mixed with the synthesized CaCl₂.6H₂O to obtain a eutectic mixture, adjusting the phase transition temperature to ensure thermal comfort inside the building. 1 wt% SrCl₂.6H₂O was added to suppress supercooling in the eutectic mixture. A combination with 0.5 wt% CMC was used to prevent phase separation. FTIR and XRD analyses confirmed that the synthesis stages of the chicken eggshell-based material were identical to the reference parameters. The FTIR results showed the appearance of characteristic absorption peaks consistent with the molecular structure of calcium carbonate in the raw material, as well as the presence of O-H and calcium chloride bands in the CaCl₂.2H₂O and CaCl₂.6H₂O phases. Meanwhile, XRD data showed a diffraction pattern identical to the reference parameters, confirming that the resulting material has high crystallinity and minimal impurities. Thermal testing using DSC showed that the synthesized material has a peak melting point of 26.3°C, which is suitable for thermal comfort applications in building walls at temperatures around 22°C–26°C. Although there was a slight decrease in enthalpy to 109.3 J/g compared to the standard laboratory-grade material’s 123.13 J/g due to the influence of CMC viscosity and the purity level of the raw materials, it is interesting to note that this enthalpy reduction is more efficient than that of commercial technical-grade materials. These results demonstrate that chicken eggshells have the potential to be an effective and economical material for the future development of sustainable PCMs. Keywords: CaCl₂.6H₂O, chicken eggshells, melting point, MgCl₂.6H₂O, phase change material (PCM)

Item Type: Thesis (Sarjana)
Additional Information: 1). Dr. Dyah Arum Wulandari, M.T. 2). Dr. Wardoyo, M.T.
Subjects: Teknologi dan Ilmu Terapan > Teknik Lingkungan, Teknik Sanitasi
Teknologi dan Ilmu Terapan > Teknik Energi
Teknologi dan Ilmu Terapan > Manufaktur
Divisions: FT > D IV Teknologi Rekayasa Manufaktur
Depositing User: Users 35104 not found.
Date Deposited: 04 Aug 2026 03:36
Last Modified: 04 Aug 2026 03:36
URI: http://repository.unj.ac.id/id/eprint/68265

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